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Covalent organic frameworks have captured the imagination of the scientific community due to their ordered pores leading to important industrial applications like storage and separation. Combined with their modular synthesis and pore engineering, COFs could become ideal candidates for nano‐separations. However, fabrication of these microcrystalline powders as continuous, crack‐free, robust films remains a cardinal challenge. Herein, we have employed a simple, slow annealing strategy to construct centimetre‐scale COF films ( Tp‐Azo and Tp‐TTA ) with micrometre thickness. The as‐synthesized films are porous (SA BET = 2033 m 2 g ‐1 for Tp‐Azo ) and chemically stable. These COFs have distinct size cutoffs (~2.7 and ~1.6 nm for Tp‐Azo and Tp‐TTA.
Despite there being numerous examples of f‐element compounds supported by cyclopentadienyl, arene, cycloheptatrienyl, and cyclooctatetraenyl ligands (C 5‐8 ), cyclobutadienyl (C 4 ) complexes remain exceedingly rare. Here, we report that reaction of [Li 2 {C 4 (SiMe 3 ) 4 }(THF) 2 ] ( 1 ) with [U(BH 4 ) 3 (THF) 2 ] ( 2 ) gives the pianostool complex [U{C 4 (SiMe 3 ) 4 }(BH 4 ) 3 ][Li(THF) 4 ] ( 3 ), where use of a borohydride and preformed C 4 ‐unit circumvents difficulties in product isolation and closing a C 4 ‐ring at uranium. Complex 3 is an unprecedented example of an f‐element half‐sandwich cyclobutadienyl complex, and it is only the second example of an actinide‐cyclobutadienyl complex, the other being an inverse‐sandwich. The U‐C di.
Kuwait Times (Kuwait) 11/14/2019 12:18
The court of cassation yesterday sentenced a bedoon, who had been earlier sentenced to death for stabbing his father to death in Rehab, to life imprisonment. The court argued that the murder was not premeditated as the suspect was only trying to stop his father from harshly beating his sister and mother. His father then […]. .
Business Insider 11/14/2019 12:17
let you earn , , and more for each dollar you spend. Some of the best cards also offer worth hundreds of dollars. Other perks to look for in cards for holiday shopping include and extended warranties. Cards at every price point — from the premium to the no-annual-fee — offer these benefits. Once you open a new credit card, make sure you're using to maximize your spending. Many credit card issuers and rewards programs offer online portals that dole out additional rewards for every dollar you spend at popular stores like Home Depot, Kohl's, and Sephora. With the holidays well on their way and your time left to shop slowly dwindling, you're probably looking for ways to save money and maximize your spending. It always makes sense to shop around.
Business Insider 11/14/2019 12:13
Elite nannies often know the households of the rich and powerful better than the parents themselves. Business Insider asked nannies what they wish their bosses knew — and they had feedback about everything from household security to their job responsibilities. One nanny was concerned about the pressure the parents' high expectations put on the kids. When you hire people to run your household, it's possible that they just might get to know how it works better than you do. Business Insider interviewed seven elite nannies to find out what they learned about the households of the rich and powerful — but were afraid to tell to their bosses.
Business Insider 11/14/2019 12:11
P&G has launched Kindra, a new direct-to-consumer brand geared at helping women navigate menopause. Kindra is the first brand to come out of , the innovation studio formed by P&G Ventures and to build new consumer-facing brands. It will operate independently of M13 and P&G's portfolio. P&G has taken a multi-pronged approach to innovation by acquiring, incubating, and now launching an independent consumer brand. The hope is that ultimately these brands can be folded back into one of P&G's six sector business units. After and , P&G is now coming after the menopause market. The consumer packaged goods giant has launched Kindra, a new direct-to-consumer brand geared at helping women navigate menopause. Kindra is the first brand to come out of ,
Forbes 11/14/2019 12:11
People expect a lot from the leaders of the world’s top companies. They have good reason to. Disruption is rampant. Economies are failing. Faith in governments is low. Meanwhile, these senior executives could be considered the master value creators of our times. They generate extraordinary returns.

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