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In hunting for safe and cost‐effective materials for post lithium‐ion energy storage systems, design and synthesis of high‐performance solid electrolytes (SEs) are currently bottlenecks for all‐solid‐state batteries. Many issues need to be addressed, such as chemical stability during processing, storing and using in ambient condition. Therefore, we investigate the effect of water as well as oxyhdryl group (▪OH) on NaBi 3 O 4 Cl 2 through evaluating ionic conductivity. It is noted that presence of water and ▪OH results in an increase in ionic conductivity of NaBi 3 O 4 Cl 2 due to the diffusion of H 2 O into NaBi 3 O 4 Cl 2 and partially forming binding ▪OH through oxygen vacancy repairing. Furthermore, Ab intio calculation reveals that the
Chiral 1,2‐bimetallic reagents are useful motifs in synthetic chemistry. Although syn ‐1,2‐bimetallic compounds can be prepared by alkene dimetallation, anti ‐1,2‐bimetallics are still rare. The stereospecific 1,2‐metallate shift that occurs during conjunctive cross‐coupling is shown to enable a practical and modular approach to the catalytic synthesis of enantioenriched anti ‐1,2‐borosilanes. In addition to reaction development, the synthetic utility of anti ‐1,2‐borosilanes was investigated, including applications to the synthesis of anti ‐1,2‐diols and anti ‐1,2‐amino alcohols.

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