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Separations Now 10/16/2019 04:12
As LC-MS is increasingly used, analysts face the problem of deciding which conditions will give the greatest ionisation efficiency, and hence the greatest sensitivity. A team from the University of Tartu (Estonia) examined a group of over 50 organic compounds in order to determine which solvent (methanol or acetonitrile) and ionisation method (ESI or APCI) gave the most efficient ionisation.
Separations Now 10/01/2019 05:31
Cashew nut shell oil has a variety of industrial uses, but improved analytical methods are needed. A team of scientists from the T.K.M. College of Arts and Science (Kollam, India) and three Egyptian institutions, the National Research Centre (Cairo), October 6 University and Kafrelsheikh University, used silyl derivatisation and GC-MS to determine the composition of cashew nut oil.
Separations Now 09/26/2019 04:56
In order to maximise its effectiveness and minimise side effects, the levels in plasma and tears of the anti-cancer drug tegafur and its active metabolite 5-fluorouracil need to be monitored. A new rapid method has been for the quantification of tegafur and 5-fluorouracil using hydrophilic interaction liquid chromatography (HILIC) and MS/MS.


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